Copia del Anexo 1 con los parámetros y ensayos habilitados por la SubSecreataría de Política Ambiental de la provincia de Buenos Aires. Laboratorio habilitado N°: 039, Resolución SPA 026/02
MATRICES, PARAMETROS, METODO Y LIMITE DE DETECCION
|
Matriz |
Analito |
Método
o Técnica |
Límite
de detección |
|
Agua |
Turbidez |
Standard
Methods for the Examination of Water and Wastewater 2130 |
0,05
NTU |
|
Agua |
pH |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,02
pH |
|
Agua |
Alcalinidad |
Standard
Methods for the Examination of Water and Wastewater 2320 |
0,01
mg/l |
|
Agua |
Dureza |
Standard
Methods for the Examination of Water and Wastewater 2340 |
0,01
mg/l |
|
Agua |
Conductividad |
Standard
Methods for the Examination of Water and Wastewater 2510 |
0.01
µS/cm |
|
Agua |
Salinidad |
Standard
Methods for the Examination of Water and Wastewater 2520 |
0,01
0/00 |
|
Agua |
Sólidos
totales |
Standard
Methods for the Examination of Water and Wastewater 2540 |
0,001
mg/l |
|
Agua |
Sólidos
totales disueltos |
Standard
Methods for the Examination of Water and Wastewater 2540 |
0,001
mg/l |
|
Agua |
Sólidos
totales en suspensión |
Standard
Methods for the Examination of Water and Wastewater 2540 |
0,001
mg/l |
|
Agua |
Sólidos
totales volátiles (550°c) |
Standard
Methods for the Examination of Water and Wastewater 2540 |
0,001
mg/l |
|
Agua |
Sólidos
sedimentables |
Standard
Methods for the Examination of Water and Wastewater 2540 |
0,001
mg/l |
|
Agua |
Olor |
Standard
Methods for the Examination of Water and Wastewater 2150 |
1
TOD |
|
Agua |
Temperatura |
Standard
Methods for the Examination of Water and Wastewater 2550 |
0.01°C |
|
Agua |
OCR
(Velocidad de consumo de oxígeno) |
Standard
Methods for the Examination of Water and Wastewater 2710 |
0,01
mg
O2/gh |
|
Agua |
Volumen
de lodo sedimentable |
Standard
Methods for the Examination of Water and Wastewater 2710 |
0,01
ml/l |
|
Agua |
Índice
de volumen de lodo |
Standard
Methods for the Examination of Water and Wastewater 2710 |
0,01
ml/g |
|
Agua |
Gravedad
específica |
Standard
Methods for the Examination of Water and Wastewater 2710 |
0,01
(T/4°C) |
|
Agua |
Tiempo
de filtrado |
Standard
Methods for the Examination of Water and Wastewater 2710 |
1
s/100 ml |
|
Agua |
Manganeso |
US
EPA FR 34193 |
0,6
mg/l |
|
Agua |
Arsénico |
US
EPA FR 206.4 |
0,04
mg/l |
|
Agua |
Cromo
total |
US
EPA I -1230-85 |
0,01
mg/l |
|
Agua |
Cobre |
US
EPA FR 36166 |
0,02
mg/l |
|
Agua |
Plomo |
US
EPA 3500 Pb D |
0,05
mg/l |
|
Agua |
Níquel |
US
EPA 3500 Ni D |
0,021
mg/l |
|
Agua |
Zinc |
US
EPA FR 36166 |
0,04
mg/l |
|
Agua |
Hierro
total |
US
EPA FR 43459 |
0,02
mg/l |
|
Agua |
Detergentes
SAM |
Standard
Methods for the Examination of Water and Wastewater 5540 |
0,05
mg/l |
|
Agua |
Cloro
residual |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,01
mg/l |
|
Agua |
Cloro
residual |
USEPA
330.5 |
0,01
mg/l |
|
Agua |
Demanda
de cloro |
Standard
Methods for the Examination of Water and Wastewater 2350 B |
0,1
mg/l |
|
Agua |
Amonio |
Standard
Methods for the Examination of Water and Wastewater 4500 US EPA |
0,06
mg/l |
|
Agua |
Nitritos |
Standard
Methods for the Examination of Water and Wastewater 4500 USEPA |
0,001
mg/l |
|
Agua |
Nitratos |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,01
mg/l |
|
Agua |
Nitrógeno
total |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,2
mg/l |
|
Agua |
N
orgánico |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,2
mg/l |
|
Agua
|
Clorofila
a |
USEPA
445.0 |
0,05
µg/l |
|
Agua |
Feofitina
a |
USEPA
445.0 |
0,06
µg/l |
|
Agua |
Oxígeno
disuelto |
Standard
Methods for the Examination of Water and Wastewater 4500 C- G |
0,1
mg/l |
|
Agua |
Fósforo
total |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,2
mg/l |
|
Agua |
Fósforo
total |
US
EPA 365.2 |
0,2
mg/l |
|
Agua |
Ortofosfatos |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,01
mg/l |
|
Agua |
Ortofosfatos |
US
EPA 365.2 |
0,01
mg/l |
|
Agua |
Sulfuro |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,01
mg/l |
|
Agua |
Sulfuro |
US
EPA 376.2 |
0,01
mg/l |
|
Agua |
Sulfatos |
Standard
Methods for the Examination of Water and Wastewater 4500 |
7
mg/l |
|
Agua |
Sulfatos |
US
EPA 375.4 |
7
mg/l |
|
Agua |
Hidrocarburos
totales |
Standard
Methods for the Examination of Water and Wastewater 5520 |
1
mg/l |
|
Agua |
DBO5 |
Standard
Methods for the Examination of Water and Wastewater 5210 |
2
mg/l |
|
Agua |
DQO |
Standard
Methods for the Examination of Water and Wastewater 5220 H 8000 US EPA |
5
mg/l |
|
Agua |
Grasas
y aceites SSEE |
Standard
Methods for the Examination of Water and Wastewater 5520 |
1
mg/l |
|
Agua |
Cloruros |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,5
mg/l |
|
Agua |
Cianuro |
Standard
Methods for the Examination of Water and Wastewater 4500 |
0,05
mg/l |
|
Agua |
Fenoles |
Standard
Methods for the Examination of Water and Wastewater 5530 – 6420 |
0,003
mg/l |
|
Agua |
Fenoles |
US
EPA 420.1 |
0,003
mg/l |
|
Agua |
Plaguicidas
organoclorados |
US
EPA 8081 a / 8270 C GC-MS |
1µg/l |
|
Agua |
Plaguicidas
organofosforados |
US
EPA 8141 a GC FID |
1
µg/l |
|
Agua |
Orgánicos
semivolátiles |
US
EPA 8270 C GC-MS |
10
µg/l |
|
Agua |
Orgánicos
volátiles |
Standard
Methods for the Examination of Water and Wastewater 6200 |
0,1
µg/l |
|
Agua |
Orgánicos
volátiles |
USEPA
8260b |
0,1
µg/l |
|
Agua |
PCB |
US
EPA 8270 C GC-MS / 8275 |
10
µg/l |
|
Agua |
Coliformes
totales |
Standard
Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
1
UFC |
|
Agua |
Coliformes
fecales |
Standard
Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
1
UFC |
|
Agua |
Ecotoxicidad
aguda sobre peces |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Agua |
Ecotoxicidad
con algas dulceacuícolas o marinas |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Agua |
Ecotoxicidad
aguda con Cladóceros Daphnia magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Agua |
Ecotoxicidad
crónica con Cladóceros Daphnia
magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Agua |
Ecotoxicidad
aguda con Anfípodos: Hyalella
curvispina y H. azteca |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Agua |
Ecotoxicidad
crónica con Anfípodos |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Residuos
(Semisólidos) |
Sólidos
totales, fijados y volátiles |
Standard
Methods for the Examination of Water and Wastewater 2540 |
0,001
mg/l |
|
Suelo |
Manganeso |
US
EPA FR 34193 |
0,6
mg/l |
|
Suelo |
Arsénico |
US
EPA FR 206.4 |
0,04
mg/l |
|
Suelo |
Cromo
total |
US
EPA I -1230-85 |
0,01
mg/l |
|
Suelo |
Cobre |
US
EPA FR 36166 |
0,02
mg/l |
|
Suelo |
Plomo |
US
EPA 3500 Pb D |
0,05
mg/l |
|
Suelo |
Níquel |
US
EPA 3500 Ni D |
0,021
mg/l |
|
Suelo |
Zinc |
US
EPA FR 36166 |
0,04
mg/l |
|
Suelo |
Hierro
total |
US
EPA FR 43459 |
0,02
mg/l |
|
Suelo
|
Sulfuro |
US
EPA 376.2 |
0,01
mg/l |
|
Suelo |
Sulfatos |
US
EPA 375.4 |
7
mg/l |
|
Suelo |
Fenoles |
US
EPA 420.1 |
0,003
mg/l |
|
Suelo |
Plaguicidas
organoclorados |
US
EPA 8081 a/ 8270 C GC-MS |
660
µg/Kg |
|
Suelo |
Plaguicidas
organofosforados |
US
EPA 8141 a GC FID |
2
µg/Kg |
|
Suelo |
Orgánicos
semivolátiles |
US
EPA 8270 C GC-MS |
660
µg/Kg |
|
Suelo |
Orgánicos
volátiles |
USEPA
8260b |
0,5
µg/Kg |
|
Suelo |
PCB |
US
EPA 8270 C GC-MS / 8275 |
660
µg/Kg |
|
Suelo |
Ecotoxicidad
con algas dulceacuícolas o marinas |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Suelo |
Ecotoxicidad
aguda con Cladóceros Daphnia magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Suelo |
Ecotoxicidad
crónica con Cladóceros Daphnia
magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Suelo |
Ecotoxicidad
aguda con Anfípodos: Hyalella
curvispina y H. azteca |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Suelo |
Ecotoxicidad
crónica con Anfípodos |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
0 |
|
Suelo |
Ecotoxicidad
elongación de raíces y germinación de semillas de lechuga Lactuca
sativa |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Suelo |
Ecotoxicidad
con lombriz de tierra Eisenia
foetida |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
0 |
|
Suelos |
Estabilidad
de barros |
CEAMSE
1987 |
0,1
mg/l |
|
Suelos |
Líquidos
libres |
CEAMSE
FR 38 |
0
mg/l |
ANEXO 2
METODOLOGIA PARA LA TOMA DE MUESTRAS
|
Matriz |
Analito |
Metodología |
|
Agua |
Turbidez |
Standard
Methods for the Examination of Water and Wastewater 2130 |
|
Agua |
pH |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Alcalinidad |
Standard
Methods for the Examination of Water and Wastewater 2320 |
|
Agua |
Dureza |
Standard
Methods for the Examination of Water and Wastewater 2340 |
|
Agua |
Conductividad |
Standard
Methods for the Examination of Water and Wastewater 2510 |
|
Agua |
Salinidad |
Standard
Methods for the Examination of Water and Wastewater 2520 |
|
Agua |
Sólidos
totales |
Standard
Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos
totales disueltos |
Standard
Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos
totales en suspensión |
Standard
Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos
totales volátiles (550°C) |
Standard
Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Sólidos
sedimentables |
Standard
Methods for the Examination of Water and Wastewater 2540 |
|
Suelo |
Estabilidad
de barros |
CEAMSE
1987 |
|
Suelo
|
Líquidos
libres |
CEAMSE
FR 38 |
|
Residuos
(semisólidos) |
Sólidos
totales, fijados y volátiles |
Standard
Methods for the Examination of Water and Wastewater 2540 |
|
Agua |
Olor |
Standard
Methods for the Examination of Water and Wastewater 2150 |
|
Agua |
Temperatura |
Standard
Methods for the Examination of Water and Wastewater 2550 |
|
Agua |
OCR
(Velocidad de consumo de oxígeno) |
Standard
Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Volumen
de lodo sedimentable |
Standard
Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Índice
de volumen de lodo |
Standard
Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Gravedad
específica |
Standard
Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Tiempo
de filtrado |
Standard
Methods for the Examination of Water and Wastewater 2710 |
|
Agua |
Manganeso |
US
EPA FR 34193 |
|
Suelo |
Manganeso |
US
EPA FR 34193 |
|
Agua |
Arsénico |
US
EPA 206.4 |
|
Agua |
Cromo
total |
US
EPA I -1230-85 |
|
Agua |
Cobre |
US
EPA FR 36166 |
|
Agua |
Plomo |
US
EPA 3500 Pb D |
|
Agua |
Níquel |
US
EPA 3500 Ni D |
|
Agua |
Zinc |
US
EPA FR 36166 |
|
Agua |
Hierro
total |
US
EPA FR 43459 |
|
Suelo |
Cromo
total |
US
EPA I -1230-85 |
|
Suelo |
Cobre |
US
EPA FR 36166 |
|
Suelo |
Plomo |
US
EPA 3500 Pb D |
|
Suelo |
Níquel |
US
EPA 3500 Ni D |
|
Suelo |
Zinc |
US
EPA FR 36166 |
|
Suelo |
Hierro
total |
US
EPA FR 43459 |
|
Agua |
Detergentes
SAM |
Standard
Methods for the Examination of Water and Wastewater 5540 |
|
Agua |
Cloro
residual |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Cloro
residual |
USEPA
330.5 |
|
Agua |
Demanda
de cloro |
Standard
Methods for the Examination of Water and Wastewater 2350 B |
|
Agua |
Amonio |
Standard
Methods for the Examination of Water and Wastewater 4500 US EPA |
|
Agua |
Nitritos |
Standard
Methods for the Examination of Water and Wastewater 4500 US EPA |
|
Agua |
Nitratos |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Nitrógeno
total |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
N
Orgánico |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Clorofila
a |
USEPA
445.0 |
|
Agua |
Feofitina
a |
USEPA
445.0 |
|
Agua |
Oxígeno
disuelto |
Standard
Methods for the Examination of Water and Wastewater 4500 C-G |
|
Agua
|
Fósforo
total |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Ortofosfatos |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Sulfuro |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Sulfatos |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua
|
Fósforo
total |
US
EPA 365.2 |
|
Agua |
Ortofosfatos |
US
EPA 365.2 |
|
Agua |
Sulfuro |
US
EPA 376.2 |
|
Suelo |
Sulfuro |
US
EPA 376.2 |
|
Agua |
Sulfatos |
US
EPA 375.4 |
|
Suelo |
Sulfatos |
US
EPA 375.4 |
|
Agua |
Hidrocarburos
totales |
Standard
Methods for the Examination of Water and Wastewater 5520 |
|
Agua |
DBO5 |
Standard
Methods for the Examination of Water and Wastewater 5210 |
|
Agua |
DQO |
Standard
Methods for the Examination of Water and Wastewater 5220 H 8000 US EPA |
|
Agua |
Grasas
y aceites SSEE |
Standard
Methods for the Examination of Water and Wastewater 5520 |
|
Agua |
Cloruros |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Cianuro |
Standard
Methods for the Examination of Water and Wastewater 4500 |
|
Agua |
Fenoles |
Standard
Methods for the Examination of Water and Wastewater 5530-6420 |
|
Agua |
Fenoles |
US
EPA 420.1 |
|
Suelo |
Fenoles |
US
EPA 420.1 |
|
Agua |
Plaguicidas
organoclorados |
US
EPA 8081a/ 8270 C |
|
Agua |
Plaguicidas
organofosforados |
US
EPA 8141 a |
|
Agua
|
Orgánicos
semivolátiles |
US
EPA 8270 C |
|
Suelo |
Plaguicidas
organoclorados |
US
EPA 8081a/ 8270 C |
|
Suelo |
Plaguicidas
organofosforados |
US
EPA 8141 a |
|
Suelo |
Orgánicos
semivolátiles |
US
EPA 8270 C |
|
Agua |
Orgánicos
volátiles |
Standard
Methods for the Examination of Water and Wastewater 6200 |
|
Agua |
Orgánicos
volátiles |
US
EPA 8260b |
|
Suelo |
Orgánicos
volátiles |
US
EPA 8260b |
|
Agua |
PCB |
US
EPA 8270 C / 8275 |
|
Suelo |
PCB |
US
EPA 8270 C / 8275 |
|
Suelo |
Liberación
de líquidos |
US
EPA 9096 |
|
Agua |
Coliformes
totales |
Standard
Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
|
Agua |
Coliformes
fecales |
Standard
Methods for the Examination of Water and Wastewater 9222 – 9223 - 9225 |
|
Agua |
Ecotoxicidad
con algas dulceacuícolas o marinas |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Agua
|
Ecotoxicidad
aguda sobre peces |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Suelo |
Ecotoxicidad
con algas dulceacuícolas o marinas |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Agua |
Ecotoxicidad
aguda con Cladóceros Daphnia magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Suelo |
Ecotoxicidad
aguda con Cladóceros Daphnia magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Agua |
Ecotoxicidad
crónica con Cladóceros Daphnia
magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Suelo |
Ecotoxicidad
crónica con Cladóceros Daphnia
magna |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Agua |
Ecotoxicidad
aguda con Anfípodos: Hyalella
curvispina y H. azteca |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Suelo |
Ecotoxicidad
aguda con Anfípodos: Hyalella
curvispina y H. azteca |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Agua |
Ecotoxicidad
crónica con Anfípodos |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Suelo |
Ecotoxicidad
crónica con Anfípodos |
US
EPA y Di Marzio WD et al. (1999)
Bulletin Environmental Contamination and Toxicology, Vol.63 (5): 654-659 |
|
Suelo |
Ecotoxicidad
elongación de raíces y germinación de semillas de lechuga Lactuca
sativa |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
|
Suelo |
Ecotoxicidad
con lombriz de tierra Eisenia
foetida |
Ecological
Effects Test Guidelines US EPA 712–C 96—164,
1996 |
ANEXO
3
LISTADO DE PERSONAL HABILITADO
CO – DIRECTOR TECNICO
|
Apellido y Nombre |
Titulo |
Matricula
Provincial |
|
DI
MARZIO, Walter Darío |
Dr.
en Ciencias Biológicas (UNLP) |
BZ 154 |
DIRECTOR TECNICO
|
Apellido
y Nombre |
Título |
Matrícula
Provincial |
|
TORTORELLI,
María del Carmen |
Dra.
En Ciencias Biológicas (UBA) |
B
BI 250 |
PERSONAL
|
Apellido
y Nombre |
Titulo Habilitante |
Matricula Provincial |
Función |
|
DI
MARZIO, Walter Darío |
Dr.
En Ciencias Biológicas (UNLP) |
BZ 154 |
Analista - Muestreo |
|
TORTORELLI,
María del Carmen |
Dra.
En Ciencias Biológicas (UBA) |
B BI 250 |
Analista - Muestreo |
|
SAENZ,
María Elena |
Dra.
En Ciencias Biológicas (UNLP) |
BE 076 |
Analista - Muestreo |
|
ALBERDI,
José Luis |
Lic.
En Ciencias Biológicas (UNLP) |
B BI 120 |
Analista - Muestreo |
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Universidad Nacional de Luján
Int. Ruta 5 y 7 - 6700 Luján - República Argentina.